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The elemental analysis of the polymer 5 did not give agreement with the calculation probably due to the contamination of HCl as the ammonium salt (Found: C, 61.67%; H, 5.42%. Calcd for (C28H28N2O8)n: C, 64.61%; H, 5.42%).
Homogeneous polymer film could not be obtained by the evacuation at higher temperature than 30°C.
L. R. Melby, R. J. Harder, W. R. Hertler, M. Mahler, R. E. Benson, and W. E. Mochel, J. Am. Chem. Soc., 84, 3374 (1962).
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Ohnishi, S., Nogami, T. & Mikawa, H. Synthesis and Electrical Resistivities of the Complexes of Alkali–Metal– TCNQ Salts with a Crown Ether Polymer. Polym J 15, 245–247 (1983). https://doi.org/10.1295/polymj.15.245
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DOI: https://doi.org/10.1295/polymj.15.245